Monday, August 27, 2012

Abstract-Terahertz Time Domain Spectroscopy of Gold Nanorod/Polymer Films




K. S. S. Christie1, 2, J. K. Young3, Y. Mukai4, W. S. Rockward1, K. Tanaka4, T. A. Searles1, T. Arikawa4
1Department of Physics, Morehouse College, Atlanta, Georgia 30314, USA
2 NanoJapan Program, Rice University, Houston, Texas 77005, USA
3 Department of Electrical & Computer Engineering, Rice University, Houston, Texas 77005, USA
4 Department of Physics, Kyoto University, Kyoto, 606-8502, Japan

 Nanoparticles have distinct electrical and vibrational properties from bulk materials originating from the quantum confinement and surface effect. Bioengineers are currently able to exploit these properties for applications in biosensing, using the surface plasmon resonance wavelength of gold nanorods to monitor changes in their local environment. THz-TDS provides scientists with new opportunities to study low frequency phonons, and low frequency phonons in gold nanoparticles are explicatory of their morphology. Here, terahertz time-domain spectroscopy (THz-TDS) was used to study the vibrational behavior of gold nanorods embedded in a poly(vinyl alcohol) matrix. The nanorods’ aspect ratios (diameter x length) of 30.7 x 81.6 nm, 30.7 x 84.0 nm, 16.2 x 39.5 nm, 18.7 x 52.2 nm, and 18.5 x 56.5 nm are confirmed by visible/near-infrared absorption spectroscopy and transmission electron microscopy. The frequencies of the phonon modes are expected to be proportional to the longitudinal and transverse sound velocity in the material and inversely proportional to the size of the Au nanorods. We discuss how THz-TDS offers a solid method to determine nanoparticle morphology

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